nkhani

N-Benzyl-N-ethylaniline

1Ndimadzimadzi onyezimira achikasu, osungunuka mu Mowa ndi ma organic solvents, osasungunuka m'madzi.

2, Njira yopanga imapezeka pochita ethyl aniline ndi benzyl chloride. Mu ketulo yokhala ndi mzere wotsogolera, onjezerani ethyl aniline, onjezerani benzyl chloride pamene mukuzizira, gwedezani kwa maola 10, kenaka muzitentha pa 100 ° C kwa maola 12. Pambuyo kutsuka ndi sodium hydroxide solution, chomalizidwacho chimapezedwa ndi vacuum distillation. Diethylaniline itha kugwiritsidwanso ntchito ngati zopangira. Chiŵerengero cha molar cha diethylaniline ndi benzyl chloride ndi 2: 1. Onjezani 1% ya kuchuluka kwa chakudya cha diethylaniline kuti muwonjezere ayodini, ikani pa 150 ℃ kwa 20h, ndi vacuum distill kuti mupeze chomaliza.

3, Amagwiritsidwa ntchito ngati utoto wapakatikati. Amagwiritsidwa ntchito popanga acidic kuwala kobiriwira SF ndi mitundu ina ya buluu.

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Nthawi yotumiza: Jul-26-2024